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排序方式: 共有2132条查询结果,搜索用时 15 毫秒
91.
Viet Hung Pham Thanh Truong Dang Tran Viet Cuong Seung Hyun Hur Byung-Seon Kong Eui Jung Kim Jin Suk Chung 《Korean Journal of Chemical Engineering》2012,29(5):680-685
We report the effect of temperature on the extent of graphene oxide reduction by hydrazine and the dispersibility of the resulting
chemically converted graphene (CCG) in polar organic solvents. The extent of graphene oxide reduction at high temperatures
was only slightly higher than at low temperatures (30–50 °C), while the dispersibility of the resulting CCG in organic solvents
decreased markedly with increasing temperature. The low dispersibility of CCGs prepared at high temperatures was greatly affected
by reduction and influenced by the formation of an irreversible agglomerate of CCG at high temperatures. The reduction of
graphene oxide at low temperatures is necessary to prepare highly dispersible CCG in organic solvents. CCG prepared at 30
°C is dispersible in N-methyl-2-pyrrolidone concentrations as high as 0.71 mg/mL. The free-standing paper made of this CCG
possessed an electrical conductivity of more than 22,000 S/m, one of the highest values ever reported. 相似文献
92.
Junghyun Kim Joon Hyuk Suh Hyun-Deok Cho Wonjae Kang Yong Seok Choi 《Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment》2016,33(3):420-432
A multi-class, multi-residue analytical method based on LC-MS/MS detection was developed for the screening and confirmation of 28 veterinary drug and metabolite residues in flatfish, shrimp and eel. The chosen veterinary drugs are prohibited or unauthorised compounds in Korea, which were categorised into various chemical classes including nitroimidazoles, benzimidazoles, sulfones, quinolones, macrolides, phenothiazines, pyrethroids and others. To achieve fast and simultaneous extraction of various analytes, a simple and generic liquid extraction procedure using EDTA-ammonium acetate buffer and acetonitrile, without further clean-up steps, was applied to sample preparation. The final extracts were analysed by ultra-high-performance liquid chromatography coupled with tandem mass spectrometry (UHPLC-MS/MS). The method was validated for each compound in each matrix at three different concentrations (5, 10 and 20 ng g–1) in accordance with Codex guidelines (CAC/GL 71-2009). For most compounds, the recoveries were in the range of 60–110%, and precision, expressed as the relative standard deviation (RSD), was in the range of 5–15%. The detection capabilities (CCβs) were below or equal to 5 ng g–1, which indicates that the developed method is sufficient to detect illegal fishery products containing the target compounds above the residue limit (10 ng g–1) of the new regulatory system (Positive List System – PLS). 相似文献
93.
94.
Taek Ho Yang Young Jang Jeong Jun Han Joon Shick Rhee 《Journal of the American Oil Chemists' Society》2001,78(3):291-296
For the synthesis of low-calorie structured lipids (LCSL), transesterification between triacetin and stearic acid using immobilized lipase in a solvent-free system was investigated. Stearic acid, a long-chain saturated fatty acid, was incorporated mainly into the sn-1 and/or sn-3 positions of triacetin by lipase-catalyzed reaction. Three types of reactor systems (open, closed, and vacuum) were studied for the production of LCSL. The effects of various reaction variables such as water activity of substrates and lipase, molar ratio of substrates, stirring speed and reaction temperature were investigated. In the vacuum reactor system, a certain amount of water was added periodically to maintain the optimal water content of the reaction system. When a suitable amount of water (0.65 wt% of substrates) was added at every 1 h into the vacuum reactor system, more than 88% LCSL was obtained within 4 h using Chirazyme® L-2. 相似文献
95.
Ah Jin Lee Bo Young Byun Dong‐Hyun Kang Juming Tang Young‐Wan Kim Han‐Joon Hwang Jae‐Hyung Mah 《International Journal of Food Science & Technology》2011,46(7):1494-1501
The objective of this study was to investigate the influence of zinc on the sporulation and viability of Clostridium sporogenes and on the growth of other bacteria. When 0.5% ZnCl2 was added to a sporulation medium, it completely inhibited C. sporogenes (PA 3679) sporulation for up to 3 weeks. At concentrations of 0.5% and 1.0%, ZnCl2 not only completely inactivated the vegetative cell viability (>7.0 Log reduction) but also significantly reduced the spore viability (<2.1 Log reduction) of C. sporogenes. Taken together, it was concluded that zinc blocks C. sporogenes sporulation by damaging (or killing) vegetative cells and probably by interfering with the biosynthesis of spore components. In addition to the inhibitory effect on the sporulation and viability of C. sporogenes, ZnCl2 was found to have a broad antimicrobial spectrum against all Gram‐positive and Gram‐negative spoilage and pathogenic bacteria tested. The minimal inhibitory concentration for inhibiting the bacteria ranged between 3.7 and 7.4 mm . Therefore, we expect that this compound or a combination thereof has a potential as a surface‐cleaning agent or disinfectant. 相似文献
96.
97.
ε‐Branched Flexible Side Chain Substituted Diketopyrrolopyrrole‐Containing Polymers Designed for High Hole and Electron Mobilities 下载免费PDF全文
A‐Reum Han Gitish K. Dutta Junghoon Lee Hae Rang Lee Sang Myeon Lee Hyungju Ahn Tae Joo Shin Joon Hak Oh Changduk Yang 《Advanced functional materials》2015,25(2):247-254
Based on the integrated consideration and engineering of both conjugated backbones and flexible side chains, solution‐processable polymeric semiconductors consisting of a diketopyrrolopyrrole (DPP) backbone and a finely modulated branching side chain (ε‐branched chain) are reported. The subtle change in the branching point from the backbone alters the π?π stacking and the lamellar distances between polymer backbones, which has a significant influence on the charge‐transport properties and in turn the performances of field‐effect transistors (FETs). In addition to their excellent electron mobilities (up to 2.25 cm2 V?1 s?1), ultra‐high hole mobilities (up to 12.25 cm2 V?1 s?1) with an on/off ratio (Ion/Ioff) of at least 106 are achieved in the FETs fabricated using the polymers. The developed polymers exhibit extraordinarily high electrical performance with both hole and electron mobilities superior to that of unipolar amorphous silicon. 相似文献
98.
Yong‐Joon Kim Jong‐Hwa Woo Myung‐Soo Kim Gershon Elber 《Computer Animation and Virtual Worlds》2015,26(3-4):423-432
We present an interactive tree modeling and deformation system that supports an efficient collision detection and avoidance using a bounding volume hierarchy of sweep surfaces. Starting with conventional tree models (given as meshes), we convert them into sweep surfaces and deform their branches interactively while detecting and avoiding collisions with many other branches. Multiple tree models (sharing the same topology) can be generated with great ease using this sweep‐based approach, and they can serve as a basis for the generation of a multiparameter family of trees. We demonstrate the effectiveness of our approach in an automatic generation of similar trees, the colonization of trees to form a forest, and the tree growth, aging, and withering simulations. Copyright © 2015 John Wiley & Sons, Ltd. 相似文献
99.
Yew Joon Tam Morvarid Akhavan Rezaei Mohd Lila Mohd Azmi Abdul Rani Bahaman Sewn Cen Lo 《分离科学与技术》2016,51(5):816-829
Univariate screening on factors affecting the purification performance of recombinant hepatitis B surface antigen (HBsAg) on ion exchange chromatography (IEC) and size exclusion chromatography (SEC) and the establishment of a two-step purification strategy were performed. Amongst four IEC adsorbents examined, the use of Q Sepharose XL IEC adsorbent under optimized conditions together with optimized SEC purification was able to efficiently purify HBsAg. An established purification strategy comprising the two techniques further demonstrated adaptability for scale-up operations with a final total purification factor (PF) of 94.82 ± 16.20, HBsAg purity of 95.48% and recovery yield of 78.07%. 相似文献
100.
Modified A-star algorithm for modular plant land transportation 总被引:1,自引:0,他引:1
Nam Kyu Kang Ho Joon Son Soo-Hong Lee 《Journal of Mechanical Science and Technology》2018,32(12):5563-5571
Many common path optimization algorithms are available. However, problems arise when a general route optimization algorithm is applied to land transportation of large cargo, such as a modular plant. The large and heavy structure of a modular plant can lead to a loss of time depending on the curve of the road. This problem is more critical when traveling through large turns, which may also cause mechanical problems. Therefore, curves are essential parameters for modular plant land transportation. In this research, we show the importance of angles in the path via multi-body dynamic simulations and finite element analysis. Based on these results, we constructed a pathfinding algorithm that considers the importance of angles. The traditional A-star algorithm considers only distance as a cost, whereas our modified A-star algorithm considers both distance and angle as costs. Our goal is to improve traditional A-star algorithms and optimize them for modular plant land transportation. 相似文献